Analysis of Chemical and Phase Transformations during the Synthesis of Glass Ceramics based on Bismuth-Barium-Borate Glass and Er : YAG

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Тек жазылушылар үшін

Аннотация

An original combination of thermal activation with exposure to a strong non-uniform electric field transforms a multicomponent solution into a precursor. The transformation of an aerosol into a finished mixture eliminates the stage of gel formation, its lengthy drying and subsequent polluting grinding, providing the molecular level of mixing of various components inherent in the sol-gel method. Using the method of synchronous thermal analysis (STA), the phase, chemical and other thermal manifestations of 1) the bismuth-barium borate part of the charge (0.2Bi2O3-0.6B2O3-0.2BaO), 2) the charge of (Er0.5Y0.5)AG components, and 3) the charge precursor, which initially combines all the necessary components of glass-ceramics, were studied. The Gibbs energy minimization method was used to determine the conditions for the formation of crystalline phases of garnet and yttrium borate, identified by X-ray phase analysis (XRD) data in glass ceramic samples formed at different temperatures from an ultrafine charge.

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Авторлар туралы

A. Plekhovich

Devyatykh Institute of Chemistry of High Purity Substances of the Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: plekhovich@ihps-nnov.ru
Ресей, Nizhny Novgorod

A. Kutyin

Devyatykh Institute of Chemistry of High Purity Substances of the Russian Academy of Sciences

Email: plekhovich@ihps-nnov.ru
Ресей, Nizhny Novgorod

K. Balueva

Devyatykh Institute of Chemistry of High Purity Substances of the Russian Academy of Sciences

Email: plekhovich@ihps-nnov.ru
Ресей, Nizhny Novgorod

E. Rostokina

Devyatykh Institute of Chemistry of High Purity Substances of the Russian Academy of Sciences

Email: plekhovich@ihps-nnov.ru
Ресей, Nizhny Novgorod

M. Komshina

Devyatykh Institute of Chemistry of High Purity Substances of the Russian Academy of Sciences

Email: plekhovich@ihps-nnov.ru
Ресей, Nizhny Novgorod

K. Shumovskaya

Devyatykh Institute of Chemistry of High Purity Substances of the Russian Academy of Sciences

Email: plekhovich@ihps-nnov.ru
Ресей, Nizhny Novgorod

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2. Fig. 1. STA curve of an ultrafine glass sample 0.2Bi2O3–0.6B2O3–0.2BaO (blue line) and glass of the same composition in the shape of a disk from the work [24] (black line). Heating speed of 10 degrees/min

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3. Fig. 2. Curves of Er0.5Y0.5AG charge samples from a hydrosol of the composition Al5(NO3)3(OH)12 × 3Y(OH)2(OOCCH3): the green lines correspond to a single-stage spray version of the synthesis of an ultrafine charge at 675 K, the pink lines correspond to a charge obtained by drying a binary hydrosol at 425 K in a drying cabinet followed by dispersion in a planetary mill

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4. Fig. 3. X-ray images of glass ceramic samples after annealing at 1150, 1240, and 1425 K. The barcodes shown correspond to Y3BO6 (ISCD 84966), YBO3 (ISCD 100015) and Y3Al5O12 (ISCD 067103)

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5. Fig. 4. Comparison of the curves of three variants of an ultrafine charge synthesized under the same conditions: 1 – glass 0.2Bi2O3–0.6B2O3–0.1), 2 – xerogel Er0.5Y0.5AG (Fig. 2) and 3 – charge precursor, initially combining all components of glass ceramics 0.46(0.2Bi2O3–0.6B2O3–0.2BaO)-0.54Er:YAG. The temperature range of spreading for curves 1 and 3 is highlighted in gray

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6. Fig. 5. Equilibrium composition of glass crystals 0.54YAG + 0.46[0.2Bi2O3–0.6B2O3–0.2BaO]. In the lower part of the figure there are separately crystallizing phases and components of the associated solution (melt)

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