Stereolithographic Fabrication of Alumina Ceramics from Aluminum Chloride-Containing Polymerizable Precursors

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An approach has been proposed for preparing polymerizable precursors to alpha-alumina and aluminum oxynitride ceramics and using them in stereolithographic fabrication of aluminum-containing ceramics. With allowance for their homogeneity (optical transmission), photopolymerizability, and weight loss during thermolysis, three precursors based on aluminum chlorides (anhydrous and hexahydrate) and a basic aluminum chloride were chosen for characterization. We analyzed the behavior of the precursors during firing in an ammonia atmosphere for the preparation of oxynitride ceramics and during firing in air for the preparation of alpha-alumina ceramics from homogeneous precursors. Stereolithographic 3D printing of alpha-alumina ceramics was tested, in particular with the use of the proposed precursors in the form of photopolymerizable binders allowing the fraction of alumina in photosuspensions to be increased.

作者简介

D. Larionov

Faculty of Materials Science, Moscow State University, 119991, Moscow, Russia

Email: valery.putlayev@gmail.com
Россия, 119991, Москва, Ленинские горы, 1, с. 73

P. Evdokimov

Faculty of Materials Science, Moscow State University, 119991, Moscow, Russia; Faculty of Chemistry, Moscow State University, 119991, Moscow, Russia

Email: valery.putlayev@gmail.com
Россия, 119991, Москва, Ленинские горы, 1, с. 73; Россия, 119991, Москва, Ленинские горы, 1, с. 3

A. Garshev

Faculty of Materials Science, Moscow State University, 119991, Moscow, Russia; Faculty of Chemistry, Moscow State University, 119991, Moscow, Russia

Email: valery.putlayev@gmail.com
Россия, 119991, Москва, Ленинские горы, 1, с. 73; Россия, 119991, Москва, Ленинские горы, 1, с. 3

D. Kozlov

Faculty of Materials Science, Moscow State University, 119991, Moscow, Russia

Email: valery.putlayev@gmail.com
Россия, 119991, Москва, Ленинские горы, 1, с. 73

V. Putlyaev

Faculty of Materials Science, Moscow State University, 119991, Moscow, Russia; Faculty of Chemistry, Moscow State University, 119991, Moscow, Russia

编辑信件的主要联系方式.
Email: valery.putlayev@gmail.com
Россия, 119991, Москва, Ленинские горы, 1, с. 73; Россия, 119991, Москва, Ленинские горы, 1, с. 3

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版权所有 © Д.С. Ларионов, П.В. Евдокимов, А.В. Гаршев, Д.А. Козлов, В.И. Путляев, 2023