Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Тек жазылушылар үшін

Аннотация

New bimetallic pivalate Pd(II) complex [PdNi(OOCtBu)4(HOOCtBu)] (I) has been synthesized from [PdNi(OOCMe)4] and used as a starting reagent in a further complexation reaction. Cyclometallated binuclear carboxylate palladium complexes [(OOCMe)Pd(2‑phpy)]2 (II) and [(OOCtBu)Pd(2‑phpy)]2 (III) have been obtained by the reaction between heterometallic compounds [Pd(OOCR)4Ni] (R = Me, tBu) and 2-phenylpyridine (2-phpy). The reaction proceeds at room temperature under mild conditions. All the compounds obtained have been isolated in crystalline form from a medium of nonpolar solvents, characterized by single-crystal X-ray diffraction analysis, and deposited at the Cambridge Crystallographic Data Center (CCDC nos. 2256606 for I, 2247942 for II, and 2247943 for III).

Авторлар туралы

Yu. Makarevich

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

M. Vargaftik

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

M. Nesterenko

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

M. Panina

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

A. Popova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

I. Skabitsky

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

O. Sulimova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

E. Sosunov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

N. Ogarkova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

I. Yakushev

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: ilya.yakushev@igic.ras.ru
119991, Moscow, Russia

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© Ю.Е. Макаревич, Н.К. Огаркова, Е.А. Сосунов, О.В. Сулимова, И.В. Скабицкий, А.С. Попова, М.В. Панина, М.Ю. Нестеренко, М.Н. Варгафтик, И.А. Якушев, 2023