Synthesis, structure and optical properties of semiconductor perovskite nanoparticles CsBX3 (B = Pb, Mn; X = Br, Cl)

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Resumo

Currently, ABX3 nanoparticles (NPs) based on lead halides attract the attention due to their unique optical properties and a wide range of applications. The preparation of NPs with lead as a partial or complete replacement is particularly interesting because of the toxicity of this chemical element and most of its compounds. In this study, we propose a modified method for perovskite NPs synthesis using manganese as a partial replacement for lead. The results obtained describe the structures, shapes and dimensions of the synthesized nanoparticles. It has been shown that partial replacement of lead with manganese leads to the appearance of new photoluminescence bands in the region of 600 nm.

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Sobre autores

V. Gushchina

Moscow Institute of Physics and Technology (National Research University); Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: ya.l2er0us0ya2012@ya.ru
Rússia, Dolgoprudny, 141701; Moscow, 119991

A. Son

Moscow Institute of Physics and Technology (National Research University); Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Autor responsável pela correspondência
Email: sonsacha@gmail.com
Rússia, Dolgoprudny, 141701; Moscow, 119991

A. Egorova

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Rússia, Moscow, 119991

A. Arkhipenko

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Rússia, Moscow, 119991

M. Teplonogova

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Rússia, Moscow, 119991

N. Efimov

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Rússia, Moscow, 119991

S. Kozyukhin

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Rússia, Moscow, 119991

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2. Рис.1. ② : 1 – cspbbr3; 2 – cspbcl3–zbrz; 3 – cspbcl3; 4 – cspb1–ymnycl3–Zbrz; 5 – Cspb1–ymnycl3.

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3. Рис. 2. Микрофотографии наночастиц различных составов: CsPbBr3 (а); CsPbCl3–zbr you (б); CsPbCl3 (в); CsPb1–yMnyCl3–zbr you (г); CsPb1–yMnyCl3 (д).

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4. Fig. 3. ② : 1 – cspbbr3; 2 – cspbcl3–zbrz; 3 – cspbcl3; 4 – cspb1–ymnycl3–zbrz; 5 – Cspb1–Ymnycl3.

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5. Fig. 4. 6-cspbbr3; 2 – cspbcl3 – zbrz; 3–cspbcl3; 4 – cspb1 – ymnycl3–zbrz; 5–cspb1 – ymnycl3.

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6. Fig. 5. Photoluminescence spectra of nanoparticles: 1 – CsPbBr3 (λvozb = 365 nm); 2 – CsPbCl3–zBrz (λvozb = = 365 nm); 3 – CsPbCl3 (λvozb = 365 nm); 4 – CsPb1–yMnyCl3–zBrz (λvozb = 227 nm); 5 – CsPb1–yMnyCl3 (λvb = 241 nm).

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7. Fig. 6. EPR spectra for CsPb1–yMnyCl3 nanoparticles (X-band, 294 K).

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